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MODULE DESCRIPTOR
Module Title
Instrumental Analytical Sciences
Reference PLM303 Version 1
Created February 2023 SCQF Level SCQF 11
Approved March 2023 SCQF Points 30
Amended August 2021 ECTS Points 15

Aims of Module
To effectively problem-solve and critically evaluate analytical techniques such as Chromatography, Electroanalysis, Microscopy, Molecular Spectroscopy, and Mass Spectrometry.

Learning Outcomes for Module
On completion of this module, students are expected to be able to:
1 Critically evaluate a range of advanced analytical instrumentation.
2 Critically discuss conventional techniques for the solution of a given analytical problem.

Indicative Module Content
The principles, applications and limitations of:- Spectroscopy - atomic spectroscopy (emission and absorption), x-ray fluorescence; molecular spectroscopy - UV/Vis, FTIR, fluorescence, raman, mass spectrometry, phosphorescence, lifetime TRF, derivative spectroscopy, NIR, FIR, NMR; Chromatography - GC, HPLC, UPLC, CZE and higher modes, HILIC, SCFC, green chromatography, GC-GC, affinity chromatography, LC-MS, GC-MS, LC-MS/MS. Microscopy - TEM, SEM/EDXA Electroanalysis - ISE's, potentiometry, voltammetry, biosensors.

Module Delivery
The module is delivered through a series of lectures and tutorials. Some guest lectures. The separate laboratory programme also affords students the opportunity to develop and extend the material in a practical context.

Indicative Student Workload Full Time Part Time
Contact Hours 48 48
Non-Contact Hours 252 252
Placement/Work-Based Learning Experience [Notional] Hours N/A N/A
TOTAL 300 300
Actual Placement hours for professional, statutory or regulatory body    

ASSESSMENT PLAN
If a major/minor model is used and box is ticked, % weightings below are indicative only.
Component 1
Type: Examination Weighting: 100% Outcomes Assessed: 1, 2
Description: Component 1 is a closed book examination.

MODULE PERFORMANCE DESCRIPTOR
Explanatory Text
The grade represents Component 1 (EX1). A minimum module grade of D is required for a pass. Non-submission of either component will result in an NS grade.
Module Grade Minimum Requirements to achieve Module Grade:
A A
B B
C C
D D
E E
F F
NS Non-submission of work by published deadline or non-attendance for examination

Module Requirements
Prerequisites for Module None in addition to the course entry requirements.
Corequisites for module None.
Precluded Modules None.

INDICATIVE BIBLIOGRAPHY
1 SKOOG, D.A., HOLLER, F.J. and CROUCH, S.A. 2017. Principles of Instrumental Analysis. Seventh Edition. Belmont, CA: Thomson Higher Education.
2 POOLE,C.F. 2021. Gas Chromatography. Second Edition. Electronic resource.
3 LAJUNEN, L.H.J. and PERAMAKI, P. 2004. Spectrochemical Analysis by Atomic Absorption and Emission. Second Edition. Cambridge, UK: The Royal Society of Chemistry.
4 SCHMIDT, W. 2005. Optical Spectroscopy in Chemistry and Life Sciences. An Introduction. Weinheim, Germany: Wiley-VCH.
5 BRETT, C.M.A. AND BRETT, A.M.O. 1998. Electroanalysis, Oxford Chemistry Primers. Oxford University Press.
6 LANGMAN, L.J. 2012. LC-MS in Drug Analysis: Methods and Protocols. Electronic Resource.
7 LEVINSON, R. 2001. More Modern Chemical Techniques. London, UK: The Royal Society of Chemistry.


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