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MODULE DESCRIPTOR
Module Title
Instrumental Analytical Sciences
Reference ASM019 Version 2
Created August 2021 SCQF Level SCQF 11
Approved February 2018 SCQF Points 30
Amended August 2021 ECTS Points 15

Aims of Module
To effectively problem-solve and critically evaluate analytical techniques such as Chromatography, Electroanalysis, Microscopy and Spectroscopy.

Learning Outcomes for Module
On completion of this module, students are expected to be able to:
1 Critically evaluate and appraise a range of advanced analytical instrumentation.
2 Critically appraise and discuss conventional techniques for the solution of a given analytical problem.
3 Demonstrate critical professional competence in oral presentations and data handling skills for the solution of a given analytical problem.

Indicative Module Content
The principles, applications and limitations of:- Spectroscopy - atomic spectroscopy (emission and absorption), x-ray fluorescence; molecular spectroscopy - UV/Vis, FTIR, fluorescence, raman, mass spectrometry, phosphorescence, lifetime TRF, derivative spectroscopy, NIR, FIR, NMR; Chromatography - GC, HPLC, UPLC, CZE and higher modes, HILIC, SCFC, green chromatography, GC-GC, affinity chromatography, LC-MS. Microscopy - TEM, SEM/EDXA Electroanalysis - ISE's, potentiometry, voltammetry, biosensors.

Module Delivery
The module is delivered through a series of lectures and tutorials. Some guest lectures. The separate laboratory programme also affords students the opportunity to develop and extend the material in a practical context.

Indicative Student Workload Full Time Part Time
Contact Hours 48 48
Non-Contact Hours 252 252
Placement/Work-Based Learning Experience [Notional] Hours N/A N/A
TOTAL 300 300
Actual Placement hours for professional, statutory or regulatory body    

ASSESSMENT PLAN
If a major/minor model is used and box is ticked, % weightings below are indicative only.
Component 1
Type: Examination Weighting: 60% Outcomes Assessed: 1
Description: Component 1 is a closed book examination.
Component 2
Type: Examination Weighting: 40% Outcomes Assessed: 2, 3
Description: Component 2 is a PowerPoint Presentation and oral assessment which appraises critical problem solving skills with respect to data analysis from a given analytical application.

MODULE PERFORMANCE DESCRIPTOR
Explanatory Text
The first grade represents Component 1 (EX1) weighted as major and the second, Component 2 (CW1), weighted as minor. A minimum module grade of D is required for a pass, with compensation of grade E in Component 1 or Component 2 permitted. Non-submission of either component will result in an NS grade.
Module Grade Minimum Requirements to achieve Module Grade:
A AA, AB
B AC, AD, BA, BB, BC, CA
C AE, BD, BE, CB, CC, CD, DA, DB, EA
D CE, DC, DD, DE, EB, EC
E AF, BF, CF, DF, ED, EE, EF, FA, FB, FC, FD
F FE, FF
NS Non-submission of work by published deadline or non-attendance for examination

Module Requirements
Prerequisites for Module None in addition to the course entry requirements.
Corequisites for module None.
Precluded Modules None.

INDICATIVE BIBLIOGRAPHY
1 SKOOG, D.A., HOLLER, F.J. and CROUCH, S.A. Principles of Instrumental Analysis. Current Edition. Belmont, CA: Thomson Higher Education.
2 MILLER, J.N. and MILLER, J.C. Statistics and Chemometrics for Analytical Chemistry. Current Edition. Essex, UK: Pearson Education Limited.
3 POOLE,C.F., Gas Chromatography. Current Edition. Electronic resource.
4 LAJUNEN, L.H.J. and PERAMAKI, P. Spectrochemical Analysis by Atomic Absorption and Emission. Current Edition. Cambridge, UK: The Royal Society of Chemistry.
5 SCHMIDT, W. Optical Spectroscopy in Chemistry and Life Sciences. An Introduction. Current Edition. Weinheim, Germany: Wiley-VCH.
6 BRETT, C.M.A. AND BRETT, A.M.O., Electroanalysis, Oxford Chemistry Primers, Current Edition. Oxford University Press.
7 LANGMAN, L.J., LC-MS in Drug Analysis, Electronic Resource; Current Edition. Methods and Protocols.
8 LEVINSON, R. More Modern Chemical Techniques. Current Edition. London, UK: The Royal Society of Chemistry.


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